Agilent Technologies 1100 Series manuály

Uživatelské manuály a uživatelské příručky pro Sítě Agilent Technologies 1100 Series.
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Tabulka s obsahem

Agilent Technologies 1100

1

LC Modules Control

1

Table of Contents

2

Introduction

4

Installation and

5

Configuration

5

Ethernet Communications

7

Configuring the Driver

10

Settings Parameter Group

13

Options Parameter Group

19

Hardware Parameter Group

21

Model Parameter Group

25

Configuring the Synopsis

26

Signal Configuration

28

Building a Method

31

Advanced Tools window:

35

(G1313)

36

Others Parameter Group

37

AutoSampler (G1329)

40

Speeds Parameter Group

41

AutoSampler (G1367)

45

Thermostat Parameter Group

46

(G1310)

51

Settings Control

52

Limits Control

53

Control Control

54

General Control

56

(G1312)

60

Program Parameter Group

63

Compartment (G1316)

66

Left Compartment Control

67

Valves Control

69

Wavelength Detector (G1314)

70

Analogs Control

72

Spectra Control

73

Wavelength Parameter Group

74

Time Table Control

75

Detector (G1315)

76

Signals Control

77

Detector (G1321)

82

Excitation Parameter Group

84

Emission Parameter Group

84

Phosphorescence Control

87

Others Control

88

Detector (G1362)

89

Peaks Parameter Group

91

Starting and Viewing an

94

Acquisition

94

Sequence

96

Running Acquisition Status

97

(G1329)

100

General Window

101

Times Window

102

Injection Window

102

Thermostat Window

103

Maintenance Window

103

(G1367)

104

Overview Window

107

Elution Window

110

Pressure Window

110

Bottles Window

111

(G1316)

122

Valve Window

125

Column Window

125

(G1314)

127

Signal Window

129

Lamps Window

130

Signals Window

133

(G1321)

135

(G1362)

138

Actuals Window

141

Running Instrument

143

Maintenance Software

143

Technologies LC 1100 Modules

144

Logbook Window

146

Tests Window

147

Injector steps test

148

Gripper Verification test

149

Actions Window

151

(G1311)

152

Counters Window

163

Appendix

178

8. Reboot the HPLC chain

184

Tabulka s obsahem

Agilent 1100 Series

1

In This Guide…

3

Contents

5

Site Requirements

8

Damaged Packaging

9

Delivery Checklist

9

Hardware Installation

11

Setting up the CAN connection

12

Software Configuration

14

Agilent 1100 Series Valves 9

15

Figure 3 Valve configuration

15

10 Agilent 1100 Series Valves

16

Operation

17

Position

18

Valve Name

19

Position Descriptions

20

Time Table

20

Next position after run

21

Display instrument actuals

21

Handheld Controller functions

22

18 Agilent 1100 Series Valves

24

2Operation

24

Maintenance, Repair, and

25

Troubleshooting

25

Status Indicators

26

Maintenance and Repair

27

G1158A, G1159A, G1160A)

28

Disassembling the valve head

30

Reassembling the valve head

31

26 Agilent 1100 Series Valves

32

Setting the EMF limit

33

Resetting the EMF counter

34

System Errors

35

CAN failure

36

Switch failure

36

Unknown Position

37

Valve Synchronization

38

Valve Applications

39

(analytical scale)

42

(preparative scale)

43

Sample enrichment

44

Sample stripping

45

Agilent 1100 Series Valves 41

47

Valve Applications 4

47

Column Selection

48

Agilent 1100 Series Valves 43

49

Tabl e 13 Capillaries

49

Solvent Selection

50

Agilent 1100 Series Valves 45

51

Table 15 Tubing

51

46 Agilent 1100 Series Valves

52

4 Valve Applications

52

Agilent Technologies

53

General Parts

54

Agilent 1100 Series Valves 49

55

*seeTa b l e 2 3 on page 52

59

54 Agilent 1100 Series Valves

60

Specifications

61

56 Agilent 1100 Series Valves

62

6 Specifications

62

58 Agilent 1100 Series Valves

64

Safety Information

65

General Safety Information

66

Safety Symbols

68

Lithium Batteries Information

69

Radio Interference

70

Sound Emission

71

Solvent Information

72

68 Agilent 1100 Series Valves

74

7 Safety Information

74

Agilent 1100 Series Valves 69

75

70 Agilent 1100 Series Valves

76

*G1156-90001*

78

Tabulka s obsahem

Agilent 1100 Series

1

Diode Array and

1

Multiple Wavelength

1

Detectors

1

In This Guide…

3

Contents

5

Installing the Detector

13

Site Requirements

14

°C/hour (3.6 °F/hour)

15

°C/hour (1.8 °F/hour)

15

Physical Specifications

16

Unpacking the Detector

17

1 Installing the Detector

18

Figure 1 Waste Tubing Parts

18

Installing the Detector 1

19

Line power switch

23

Status indicator

23

How to optmize the Detector

29

Optimization Overview

31

2 How to optmize the Detector

32

Figure 7 Choosing a Flow Cell

32

Flow Cell Path Length

33

Peak width (response time)

35

Bandwidth

38

Slit Width

39

Options for storing spectra

42

Threshold

43

Optimizing Selectivity

44

Status Indicators

50

Error Messages

50

Wavelength Recalibration

50

Test Funct io ns

50

Timeout

54

Shutdown

55

Remote Timeout

56

Synchronization Lost

57

Leak Sensor Open

60

Leak Sensor Short

61

Compensation Sensor Open

62

Compensation Sensor Short

63

Fan Failed

64

Open Cover

65

Cover Violation

66

Visible Lamp Current

67

Visible Lamp Voltage

68

Communication Error

69

Calibration Values Invalid

70

Diode Current Leakage

71

Holmium Oxide Test Failed

72

UV Lamp Current

73

UV Lamp Voltage

74

UV Ignition Failed

75

UV Heater Current

76

Module Type Changed

78

Type B, Parameter 1 or 3

79

Assembly

80

Heater Failed

82

Heater Power At Limit

83

Test Functions

85

Holmium Oxide Test

86

Test Failed

87

Intensity Test

88

Intensity Test Evaluation

89

Cell Test

90

Dark-Current Test

91

Filter Test

93

Repairing the Detector

95

Cleaning the Detector

97

Using the ESD Strap

98

4 Repairing the Detector

100

Figure 29 Main Assemblies

100

Simple Repairs

101

Exchanging a Lamp

102

• Turn the lamp on

104

Exchanging a Flow Cell

105

• Replace the front cover

107

• Turn off the flow

108

• Remove the front cover

108

• Perform a leak test

111

• Insert the flow cell

111

Repairing the Detector 4

117

Next steps:

118

• Turn on the flow

129

Correcting Leaks

130

• Turn off the lamp(s)

132

• Replace both lamps

134

Exchanging Internal Parts

138

• Turn off the detector

140

• Disconnect the power cable

140

• Disconnect capillaries

140

AIRFLOW

149

G1315/65A

153

G1315/65B

153

Exchanging the Power Supply

164

Exchanging the Leak Sensor

167

Replacing Status Light Pipe

170

Assembling the Main Cover

178

Replacing the Interface Board

179

Agilent Technologies

181

Overview of Main Assemblies

182

Table 8 Main Assemblies

183

Optical Unit Assembly

184

Figure 36 Optical Unit Parts

185

Standard Flow Cell

186

Semi-Micro Flow Cell

188

High Pressure Flow Cell

190

Nano Flow Cells

192

Table 1 4 Generic Parts

193

Fan Assembly Parts

196

Holmium Oxide Filter

197

Coupling Lens Assembly

198

Cell Support Assembly

200

Control Module

201

Plastic Parts

204

Power and Status Light Pipes

206

Leak Parts

207

Accessory Kit

208

Figure 55 Waste Tubing Parts

209

Cable Overview

210

Analog Cables

212

Agilent 1100 to BNC Connector

213

Remote Cables

215

BCD Cables

220

Auxiliary Cable

222

CAN Cable

223

External Contact Cable

224

RS-232 Cable Kit

225

LAN Cables

226

Introduction to the Detector

227

Optical System Overview

229

Electrical Connections

232

Instrument Layout

234

EMF Counters

235

Using the EMF Counters

235

Setting the EMF Limits

236

Electronics

237

Main processor

238

SIMM Memory Module

239

Firmware

239

Leak Sensor

239

Fan Drive

239

On-board Battery

239

SCI Board

241

A/D Converter

241

PFP (PDA Front-end Processor)

241

Analog Outputs

241

Igniting the Deuterium Lamp

243

Tungsten Lamp Voltage Control

243

Diagnostic A/D Converter

245

Safety Switches

245

Interfaces

245

Temperature Control

245

Firmware Description

246

Firmware Updates

247

Subtract Dark Signal

248

Gain Correction

248

Rawdata File

251

Peak Detector

251

Optional Interface Boards

253

Recommended Cables

255

Analog Signal Output

257

GPIB Interface

257

CAN Interface

257

Remote Interface

257

Figure 65 RS-232 Cable

260

GPIB Default Addresses

262

Forced Cold Start Settings

264

Stay-Resident Settings

265

1100 DAD and MWD

269

The Analysis screen

272

Lamp ON/OFF

272

Setup View

273

Settings

274

Settings - Timetable

276

Settings - Analog

277

Settings - Spectrum Range

278

Settings - Run times

278

Signal plot

280

Method screens

281

System screen

282

System - Control

282

System - Configuration

283

Records screen

284

System / Error Log

284

Info Log

285

Firmware Update

286

Changing the serial number

288

Maintenance activities

289

Diagnostics and Tests

290

Wavelength Calibration

291

Slit Test

293

Specifications

295

Performance Specifications

296

8 Specifications

298

Safety Information

299

General Safety Information

300

Safety Symbols

302

Lithium Batteries Information

303

A Safety Information

304

Radio Interference

305

Sound Emission

306

UV-Radiation

307

Solvent Information

308

*G1315-90005*

318

Tabulka s obsahem

Agilent 1100 Series

1

Quaternary Pump

1

Reference Manual

1

Contents

10

Radio Interference 264

11

Sound Emission 264

11

Solvent Information 265

11

1 Installing the Pump

13

Site Requirements

14

Bench Space

15

Environment

15

°C (41–131 °F)

16

°C (-4–158 °F)

16

°C (77–104 °F)

16

Unpacking the Quaternary Pump

17

ESD: Electrostatic Discharge

18

Power Switch

22

Serial number

22

Installing the Pump

27

2 Optimizing Performance

31

Optimizing Performance

33

Procedure” on page 112)

33

Degasser

36

Gradient Valve (MCGV)

37

When to Use Alternative Seals

39

Optimize the Compressibility

40

Compensation Setting

40

3 Troubleshooting and

43

Test Functions

43

Troubleshooting and Test

44

Functions

44

Status Indicators

45

Power Supply Indicator

46

Pump Status Indicator

46

Error Messages

47

Timeout

48

Shut-Down

49

Remote Timeout

50

Synchronization Lost

51

Leak Sensor Open

53

Leak Sensor Short

54

Compensation Sensor Open

55

Compensation Sensor Short

56

Fan Failed

57

Open Cover

58

Restart Without Cover

59

Zero Solvent Counter

60

Pressure Above Upper Limit

61

Pressure Below Lower Limit

62

Pressure Signal Missing

63

Missing Pressure Reading

64

Pump Configuration

65

Valve Fuse

66

Inlet-Valve Fuse

67

Valve Failed

68

Motor-Drive Power

69

Encoder Missing

70

Inlet-Valve Missing

71

Temperature Out of Range

72

Temperature Limit Exceeded

73

Servo Restart Failed

74

Pump Head Missing

75

Index Limit

76

Index Adjustment

77

Index Missing

78

Stroke Length

79

Initialization Failed

80

Wait Timeout

81

Pressure Test

82

Positioning the blank nut

83

Running the Pressure Test

84

Evaluating the Results

86

Leak Test

88

Running the Leak Test

90

All plateaus negative

94

Ramp 3 does not reach limit

95

4 Repairing the Pump

97

Cleaning the Quaternary Pump

99

Using the ESD Strap

100

Overview

101

Simple Repair Procedures

102

Valve cartridge

104

Valve body

104

Repairing the Pump

105

Gold seal

106

Plastic cap

106

Purge Valve

108

Purge valve

109

Pump outlet capillary

109

Waste tube

109

Head Assembly

110

Wear-in Procedure

112

Seal Wear-in Procedure

113

Exchanging the Plungers

115

Pump head screws

116

Pump head

116

Lock screw

116

Exchanging the Wash Seals

119

Insert tool

120

Support ring

120

Plunger housing

121

Balls of spindle drive

122

Metering drive

122

Pumphead screws

122

Valve (MCGV)

123

BCD (Interface) board

126

Exchanging Internal Parts

127

Clip fastener (1)

128

Light light switch

130

Top foam cover

130

Foam lever

130

Board (LPM Board)

131

Screws and Nut

132

Analog output

132

Board recessBoard recess

132

Entering the Type Command

134

Entering the Serial Number

135

Exchanging the Damper

138

Reconnect

140

Exchanging the Fan

141

Figure 22 Exchanging the Fan

142

Exchanging the Pump Drive

143

Exchanging the Power Supply

147

Power supply screws

148

Light pipe

149

Exchanging the Leak Sensor

152

Assembling the Main Cover

155

Light switch

156

Holding

157

Leak funnel

158

Waste tube holder

158

5 Parts and Materials

159

Overview of Main Assemblies

160

Parts and Materials

161

Control Module (B-version)

163

Solvent Cabinet

164

Bottle Head Assembly

165

Hydraulic Path

166

Cover Parts

167

Sheet Metal Kit

168

Foam Parts

169

Power and Status Light Pipes

170

Leak Parts

171

Pump Head Assembly

172

Figure 35 Pump Head Assembly

173

Outlet Ball Valve Assembly

176

Purge Valve Assembly

177

Active Inlet Valve Assembly

178

Accessory Kit G1311-68705

179

Reorder number (pack of 3)

180

Reorder number (pack of 10)

180

Cable Overview

181

Analog Cables

183

Agilent 1100 to BNC Connector

184

Remote Cables

185

BCD Cables

190

Auxiliary Cable

192

CAN Cable

192

External Contact Cable

193

RS-232 Cable Kit

194

LAN Cables

195

6 Introduction to the

197

Quaternary Pump

197

How does the Pump Work?

200

Electrical Connections

204

Instrument Layout

206

EMF Counters

207

Using the EMF Counters

208

The Electronics

209

Firmware Description

214

Firmware Updates

215

Optional Interface Boards

216

LAN Board

217

Analog Signal Output

219

GPIB Interface

219

CAN Interface

219

APG Remote Interface

220

Instrument

222

GPIB Default Addresses

224

Forced Cold-Start Settings

226

Stay Resident Settings

226

Mode Select12345678

227

TEST/BOOT11001000

227

7 Control Module Screens

231

Diagnostics and Tests

251

8 Specifications

253

Performance Specifications

254

Specifications

255

Warranty Statement

257

Safety Information

260

Safety Symbols

261

Lithium Batteries Information

263

Radio Interference

264

Sound Emission

264

Solvent Information

265

In This Book

272

Tabulka s obsahem

Agilent 1100 Series

1

Capillary LC System

1

In This Manual…

3

Contents

5

Agilent Technologies

11

Site Requirements

12

Bench Space

13

Environment

13

Physical Specifications

14

System Installation Process

16

Install the Solvent Cabinet

23

Micro Well-plate Sampler)

26

Purging the Pump

34

Inject the Check-out Sample

36

Procedure

37

Optimizing Performance

39

Pump issues

40

Fused Silica Capillary issues

41

Sampler issues

42

Column thermostat issues

42

DAD issues

42

Cleaning the Solvent Filters

45

When to use Alternative Seals

47

Static Mixer and Filter

50

How the Function Works

53

Capillaries and Fittings

55

Capillary Flow Diagram

56

Capillaries and Fittings 3

57

* 2.2 12 5065-9906

61

* 1.4 7.6 G1375-87313

61

Fittings and Ferrules

62

Basic System Troubleshooting

65

Symptoms:

66

Poor peak shape

71

Wandering Detector Baseline

73

Parts and Materials

75

Micro Vacuum Degasser

76

Capillary Pump

79

Capillary Pump Hydraulic Path

82

Pump-Head Assembly

84

Figure 9 Pump head assembly

85

Capillary pump cover parts

86

Micro Well-plate Sampler

87

Thermostat for 1100 Samplers

98

5 Parts and Materials

100

Parts and Materials 5

101

Vial Trays

104

Micro Column Switching Valve

107

Diode Array Detector

111

DAD - Optical Unit Assembly

113

Figure 30 Optical Unit Parts

114

500 nl Flow Cell

115

Fan Assembly Parts

117

Holmium Oxide Filter

118

Common Parts

120

Rear panel

121

Power and Status Light Pipes

122

Leak Parts

123

Foam parts

124

Sheet metal kit

124

Micro Degasser Accessory Kit

125

Capillary Pump Accessory Kit

126

G1316-68725

129

DAD Accessory Kit

130

Tabl e 61 Cables overview

131

Analog Cables

133

Remote Cables

134

BCD Cables

140

Auxiliary Cable

142

CAN Cable

142

External Contact Cable

143

RS-232 Cable Kit

144

LAN Cables

144

Options 6

147

6Options

152

Frequency If valve leaks

156

9/64 inch hex key

156

• Disconnect the power cable

157

• Disconnect capillaries

157

Features

163

Performance Specification

163

Installation of the Flow Cell

166

~ 0.3 mm clearance

167

Replacing or Cleaning Parts

171

Performance Specifications

175

7 Performance Specifications

176

Performance Specifications 7

177

Autosampler

179

Compartment

181

Safety Information

185

Operation

186

Safety Symbols

187

Lithium Batteries Information

188

Danish Information:

188

Radio Interference

189

Sound Emission

189

Solvent Information

189

' %%(&'

196





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